A Convenient and Practical Method for the Synthesis of Aromatic Nthiophosphoryl Imines

Xinyuan Xu; Chungui Wang; Zhenghong Zhou; Zebing Zeng; Xinpeng Ma; Guofeng Zhao; Chuchi Tang

doi:10.2174/157017806778559446

ISSN: 1570-1786
E-ISSN: 1875-6255

A Convenient and Practical Method for the Synthesis of Aromatic Nthiophosphoryl Imines
Authors: Xinyuan Xu¹, Chungui Wang², Zhenghong Zhou³, Zebing Zeng⁴, Xinpeng Ma⁵, Guofeng Zhao⁶ and Chuchi Tang⁷
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¹ State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China. ² State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China. ³ State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China. ⁴ State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China. ⁵ State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China. ⁶ State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China. ⁷ State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China.
Source: Letters in Organic Chemistry, Volume 3, Issue 8, Aug 2006, p. 640 - 642
DOI: https://doi.org/10.2174/157017806778559446
- Available online: 01 Aug 2006

Abstract

Thermal condensation of acetals with different thiophosphoramides at 120-160 °C resulted in the formation of the corresponding N-thiophosphoryl imines in good to excellent yield (80-98%) with high purity (>95%, determined by 1H NMR and elemental analyses).

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2006-08-01

2025-11-08

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Article Type: Research Article

Keyword(s): acetal; N-Thiophosphoryl imine; thermal condensation; thiophosphoramide

A Convenient and Practical Method for the Synthesis of Aromatic Nthiophosphoryl Imines

Abstract

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