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- ISSN: 1570-1786
- E-ISSN: 1875-6255
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Efficient Synthesis of Wang Resin-Supported 6-O-Benzylallosamizoline
- Source: Letters in Organic Chemistry, Volume 7, Issue 5, Jul 2010, p. 396 - 398
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- 01 Jul 2010
Abstract
An efficient procedure of flash heating by microwave irradiation was described for the attachment of 6-O-benzylallosamizoline 8 to chloromethylated Wang resin 7 via its corresponding stannylene intermediate. The reaction rate and loading for compound 8 were significantly enhanced when the microwave irradiation protocol was compared with the conventional heating method.
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