Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O

Chun-juan Shi; Jianbo Zhang; Jie Fu; Jie Tang

doi:10.2174/157017806779468013

ISSN: 1570-1786
E-ISSN: 1875-6255

Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O
Authors: Chun-juan Shi¹, Jianbo Zhang², Jie Fu³ and Jie Tang⁴
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¹ Department of Chemistry, East China Normal University, Shanghai 200062, China. ² Department of Chemistry, East China Normal University, Shanghai 200062, China. ³ Department of Chemistry, East China Normal University, Shanghai 200062, China. ⁴ Department of Chemistry, East China Normal University, Shanghai 200062, China.
Source: Letters in Organic Chemistry, Volume 3, Issue 12, Dec 2006, p. 932 - 935
DOI: https://doi.org/10.2174/157017806779468013
- Available online: 01 Dec 2006

Abstract

Several monosaccharides were peracetylated in excellent isolated yields (89-100%) with vinyl acetate in aqueous Na3PO4. The per-O-acetylation reaction is fast and mild, as well as insensitive to water. Meanwhile, the workup is convenient and the catalyst can be recycled easily.

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2006-12-01

2025-10-13

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Article Type: Research Article

Keyword(s): Acetylation; catalyst; monosaccharide; sodium phosphate; vinyl acetate

Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O

Abstract

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